Aspirin

Synthesis of acetylsalicylic acid (Acetylsalicylic acidulated) Objective: * To synthesize aspirin utilisation salicylic Acid and acetic anhydride. * To calculate %yield of aspirin. Theory: * acetylsalicylic acid is the most common salicylate. It is an analgesic, antipyretic and anti-inflammatory drug that is expend in medicine nowadays. * The process involves mixing salicylic acid with acetic anhydride in a mixture while adding backbreaking sulphuric acid (catalyst). * A boost in the temperature is observed indicating that the response is taking place. Upon the drop of this temperature the reaction is close to completion. * %yield = [mass(actual) mass( hypothetic) / mass( divinatory)] x100 visible(a): 1. Erlyne Meyer Flask 2. Beakers 3. Spatula 4. Digital balance 5. Ice bath 6. suck filtration apparatus 7. Funnel paper Procedure: 1. In an potential drop add 3g of salysilic acid. 2. Add 6mL of acetic anhydride. 3. Add 10 drops of concentrated sulfuric acid. 4. Stir the mixture continuously for 10 minutes. (note the rise in temperature) 5. Add 50mL of cold water when the temperature decreases fully. 6. aplomb in ice and then filter using sucking filtration. 7. number the mass of the aspirin.

Table of Data: Reagent| Molar bunch (g/mol)| Grams (g)| Moles (mol)| Salicylic Acid| 138| 3.06g| 0.022| Acetic Anhydride| 102| -| -| The limiting reagent is Salicylic Acid since in the science research lab manual it was given that acetic anhydride is in excess. Therefore, the mass of th eoretical Aspirin = 3.06g (1:1 ratio/stoichi! ometry) Calculations: n (salicylic acid) = m/MM = 3.06/138 = 0.22 mol * n (aspirin)theoretical = 0.22 mol m (aspirin)theoretical = 3.06 g Questions: 1. The slag most apparent present would be salicylic acid. If consumed by reality it would cause monetary value to the stomach and digestive constitution due to high acidity. 2. The reaction that takes place in the personify: 3. The polymer...If you want to get a full essay, order it on our website: BestEssayCheap.com

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